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Efficient phosphine-mediated formal C(sp 3 )-C(sp 3 ) coupling reactions of alkyl halides in batch and flow.
Chemical Communications : Chem Comm 2017 May 3
The construction of C(sp3 )-C(sp3 ) bond is an essential chemical transformation in synthetic chemistry due to its abundance in organic scaffolds. Here we demonstrate a valuable adaptation of the Wittig-type chemical procedure to efficiently facilitate C(sp3 )-C(sp3 ) bond formation utilizing a range of alkyl building blocks. Additionally the method is amenable with flow synthesis to afford coupled products in good to excellent yields without laborious purification process.
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