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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Nickel-Catalyzed Aminoxylation of Inert Aliphatic C(sp 3 )-H Bonds with Stable Nitroxyl Radicals under Air: One-Pot Route to α-Formyl Acid Derivatives.
Organic Letters 2017 April 8
Nickel-catalyzed aminoxylation of an unactivated C(sp3 )-H bond with a stable nitroxyl radical has been accomplished for the first time to offer various N-alkoxyamine derivatives, which further enables a one-pot approach to α-formyl acid derivatives. The aminoxylation process reported also provides direct evidence for the oxidative addition of a cyclometallic intermediate with a free radical, which is helpful for the reaction-mechanism study in transition-metal-catalyzed functionalization of inert C(sp3 )-H bonds.
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