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Journal Article
Research Support, U.S. Gov't, Non-P.H.S.
Computationally Aided Absolute Stereochemical Determination of Enantioenriched Amines.
Organic Letters 2017 March 18
A simple and efficient protocol for sensing the absolute stereochemistry and enantiomeric excess of chiral monoamines is reported. Preparation of the sample requires a single-step reaction of the 1,1'-(bromomethylene)dinaphthalene (BDN) with the chiral amine. Analysis of the exciton coupled circular dichroism generated from the BDN-derivatized chiral amine sample, along with comparison to conformational analysis performed computationally, yields the absolute stereochemistry of the parent chiral monoamine.
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