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Counterion-induced crystallization of intermetalloid Matryoshka clusters [Sb@Pd 12 @Sb 20 ] 3-,4 .
Two intermetalloid Matryoshka cluster anions [Sb@Pd12 @Sb20 ]3-,4- obtained from the reaction of KSb and Pd(PPh3 )4 were isolated as [K(2,2,2-cryptand)]+ and [K(18-crown-6)]+ salt, respectively, and characterized by X-ray crystallography, EPR measurement and DFT theoretical calculations.
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