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Journal Article
Research Support, U.S. Gov't, Non-P.H.S.
The Conversion of tert-Butyl Esters to Acid Chlorides Using Thionyl Chloride.
Journal of Organic Chemistry 2017 March 18
The reaction of tert-butyl esters with SOCl2 at room temperature provides acid chlorides in unpurified yields of 89% or greater. Benzyl, methyl, ethyl, and isopropyl esters are essentially unreactive under these conditions, allowing for the selective conversion of tert-butyl esters to acid chlorides in the presence of other esters.
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