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Rethinking the Claisen-Tishchenko Reaction.
Angewandte Chemie 2017 January 10
Pincer-type complexes [OsH2 (CO){PyCH2 NHCH2 CH2 NHPtBu2 }] and [OsH2 (CO){HN(CH2 CH2 PiPr2 )2 }] catalyze the disproportionation reaction of aldehydes via an outer-sphere bifunctional mechanism achieving turnover frequencies up to 14 000 h(-1) . The N-H group of the catalysts is a key player in this process, elucidated with the help of DFT calculations.
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