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Isolation of a Reactive Cyclopropane Intermediate via a Unique Catalyst-Free Spontaneous Cyclopropanation Step at 0 °C.
Chemistry : a European Journal 2017 May 3
A remarkably mild, catalyst-free cyclopropanation reaction is confirmed by low-temperature isolation of a fused bicyclic cyclopropane intermediate. This intermediate is one of two that were isolated and fully characterised in a three-step temperature-controllable reaction cascade.
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