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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Regiochemically Controlled Synthesis of a β-4-β' [70]Fullerene Bis-Adduct.
Journal of Organic Chemistry 2017 January 21
A β-4-β' C70 bis-adduct regioisomer and an uncommon mono-adduct β-malonate C70 derivative were synthesized by using a Diels-Alder cycloaddition followed by an addition-elimination of bromo-ethylmalonate and a retro-Diels-Alder cycloaddition reaction. We also report the regioselective synthesis and spectroscopic characterization of Cs -symmetric tris- and C2v -symmetric tetra-adducts of C70 , which are the precursors of the mono- and bis-adduct final products.
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