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Real-time analysis of Pd 2 (dba) 3 activation by phosphine ligands.
Chemical Communications : Chem Comm 2017 January 11
A combination of UV-Vis spectroscopy and electrospray ionization mass spectrometry is used for real-time monitoring of Pd2 (dba)3 activation with sulfonated versions of PPh3 and Buchwald-type ligands. This provides insight into the effect of ligand and preparation conditions on activation and allows for establishment of rational activation protocols.
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