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Synthesis and crystal structure of tri-carbonyl-chlorido-{1-[(pyridin-2-yl-methyl-idene)amino]-adamantane}rhenium(I).
Acta Crystallographica. Section E, Crystallographic Communications 2016 September 2
The title compound, [ReCl(pyAm)(CO)3], where pyAm is 1-[(pyridin-2-yl-methyl-idene)amino]-adamantane (C16H20N2), was synthesized from the reaction of [ReCl(CO)5] and pyAm in an equimolar ratio. The Re(I) atom resides in an octa-hedral C3ClN2 coordination sphere. The Re-C bond trans to the chloride ligand is noticeably longer compared to the other two Re-C distances. Weak C-H⋯Cl hydrogen-bonding inter-actions consoldiate the packing of the mol-ecules. In this design, the pyAm ligand was employed due to its well-known pharmacokinetic properties.
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