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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
RESEARCH SUPPORT, U.S. GOV'T, NON-P.H.S.
Copper-Catalyzed Bromination of C(sp 3 )-H Bonds Distal to Functional Groups.
Angewandte Chemie 2017 January 3
Selective bromination of γ-methylene C(sp3 )-H bonds of aliphatic amides and δ-methylene C(sp3 )-H bonds of nosyl-protected alkyl amines are developed using NBS as the brominating reagent and catalytic amount of CuII /phenanthroline complexes as the catalyst. Aryl and benzylic C-H bonds at other locations remain intact during this directed radical abstraction reaction.
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