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Spin-labelled diketopiperazines and peptide-peptoid chimera by Ugi-multi-component-reactions.

Haider N Sultani, Haleh H Haeri, Dariush Hinderberger, Bernhard Westermann
Organic & Biomolecular Chemistry 2016 December 29
For the first time, spin-labelled coumpounds have been obtained by isonitrile-based multi component reactions (IMCRs). The typical IMCR Ugi-protocols offer a simple experimental setup allowing structural variety by which labelled diketopiperazines (DKPs) and peptide-peptoid chimera have been synthesized. The reaction keeps the paramagnetic spin label intact and offers a simple and versatile route to a large variety of new and chemically diverse spin labels.

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