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Configurationally Stable Chiral Dithia-Bridged Hetero[4]helicene Radical Cation: Electronic Structure and Absolute Configuration.

Bettina D Gliemann, Ana G Petrovic, Eva M Zolnhofer, Pavlo O Dral, Frank Hampel, Georg Breitenbruch, Philipp Schulze, Vijay Raghavan, Karsten Meyer, Prasad L Polavarapu, Nina Berova, Milan Kivala
Chemistry, An Asian Journal 2017 January 4
A stable chiral hetero[4]helicene radical cation was synthesized and characterized by UV/Vis absorption and EPR spectroscopy, as well as X-ray crystallography. For the first time, a combination of chiroptical methods involving ECD, ORD, and VCD, supported by quantum mechanical predictions, enabled the elucidation of the absolute configuration of such open-shell helical species.

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