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Nickel-Catalyzed Facile [2+2+2] Cyclotrimerization of Unactivated Internal Alkynes to Polysubstituted Benzenes.
Chemistry, An Asian Journal 2017 January 4
A catalytic [2+2+2] cyclotrimerization of unactivated internal alkynes providing cyclotrimerization products in excellent yields with high regioselectivity is described. The transformation is accomplished by using a simple catalytic mixture comprising Ni(acac)2 , an imidazolium salt and a Grignard reagent at room temperature or 60 °C for 20 min or 1 h.
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