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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
RESEARCH SUPPORT, U.S. GOV'T, NON-P.H.S.
Uranium(iii) and thorium(iv) alkyl complexes as potential starting materials.
Chemical Communications : Chem Comm 2016 December 14
The synthesis and characterisation of a rare U(iii) alkyl complex, U[η4 -Me2 NC(H)C6 H5 ]3 , using the dimethylbenzylamine (DMBA) ligand has been accomplished. While attempting to prepare the U(iv) compound, reduction to the U(iii) complex occurred. In the analogous Th(iv) system, C-H bond activation of a methyl group of one dimethylamine was observed yielding Th[η4 -Me2 NC(H)C6 H5 ]2 [η5 -(CH2 )MeNC(H)C6 H5 ] with a dianionic DMBA ligand. The utility of these complexes as starting materials has been analyzed using a bulky dithiocarboxylate ligand to yield tetravalent actinide species.
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