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Journal Article
Research Support, Non-U.S. Gov't
Silver-Catalyzed Cyclization of Sulfonyl Allenes to Dihydrofurans.
Organic Letters 2016 November 5
Treatment of α-hydroxy allenic sulfones with 10 mol % of silver fluoride in acetonitrile at ambient temperature furnished the corresponding 3-tosyl 2,5-dihydrofurans in excellent yields via a 5-endo-trig cyclization. The starting α-hydroxy allenic sulfones were prepared by lithiation of allenic sulfones and trapping with carbonyl compounds.
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