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JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
Access to the Phosphorylindenopyrazole Scaffold via a Metal-Free Domino Reaction of Diazoalkylphosphonates with 3-Bromophthalides.
Journal of Organic Chemistry 2016 November 19
A novel strategy is reported here for the synthesis of an indenopyrazole scaffold bearing a phosphonate group. The entire sequence includes nucleophilic addition-elimination, Seyferth-Gilbert homologation, transphosphorylation, and a 1,3-dipolar cycloaddition reaction of diazoalkylphosphonates in a perfect "domino" manner.
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