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Synthesis of a Crushed Fullerene C60H24 through Sixfold Palladium-Catalyzed Arylation.

Ruth Dorel, Paula de Mendoza, Pilar Calleja, Sergio Pascual, Esther González-Cantalapiedra, Noemí Cabello, Antonio M Echavarren
European Journal of Organic Chemistry 2016 July
The synthesis of a new C3v -symmetric crushed fullerene C60H24 (5) has been accomplished in three steps from truxene through sixfold palladium-catalyzed intramolecular arylation of a syn-trialkylated truxene precursor. Laser irradiation of 5 induces cyclodehydrogenation processes that result in the formation of C60, as detected by LDI-MS.

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