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Catalytic cyclization and competitive deactivation with Ru(P R 2 N R' 2 ) complexes.
The first successful use of the PR 2 NR' 2 (1,5-R'-3,7-R-1,5-diaza-3,7-diphosphacyclooctane) ligand family toward an organic synthesis is described. The precatalysts [Ru(Cp)(PR 2 NBn 2 )(MeCN)]PF6 are active toward cyclization of 2-ethynylbenzyl alcohol at low catalyst loading and mild temperatures. Catalyst performance however is limited by both low conscription and by competitive deactivation.
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