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Journal Article
Research Support, Non-U.S. Gov't
Cobalt-Catalyzed Monoselective Ortho-C-H Functionalization of Carboxamides with Organoaluminum Reagent.
Organic Letters 2016 November 5
A simple triphenylphosphine-ligated cobalt catalyst is reported for the direct ortho-C-H methylation and ethylation of aromatic, heteroaromatic, alkenyl, and even aliphatic carboxamides with inexpensive organoaluminum reagents in the presence of a cheap alkyl chloride as oxidant. This reaction shows monoselectivity in contrast with previously established C-H methylation methodologies.
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