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Ambiguous electrocatalytic CO 2 reduction behaviour of a nickel bis(aldimino)pyridine pincer complex.
The electrochemical properties of two Ni(NNN)X2 pincer complexes are reported where X = Cl or Br and NNN is N,N'-(2,6-diisopropylphenyl)bis-aldiminopyridine. Cyclic voltammetry under 1 atm of CO2 suggests electrocatalytic CO2 reduction activity, however, bulk electrolysis shows a poor Faradaic efficiency for CO evolution with a high Faradaic yield for H2 evolution.
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