JOURNAL ARTICLE
RESEARCH SUPPORT, NON-U.S. GOV'T
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Iterative Synthesis of Oligo[n]rotaxanes in Excellent Yield.

We present an operationally simple iterative coupling strategy for the synthesis of oligomeric homo- and hetero[n]rotaxanes with precise control over the position of each macrocycle. The exceptional yield of the AT-CuAAC reaction, combined with optimized conditions that allow the rapid synthesis of the target oligomers, opens the door to the study of precision-engineered oligomeric interlocked molecules.

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