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Synthetic Studies toward the C14-C29 Fragment of Mirabalin.

Johan Cornil, Pierre-Georges Echeverria, Sébastien Reymond, Phannarath Phansavath, Virginie Ratovelomanana-Vidal, Amandine Guérinot, Janine Cossy
Organic Letters 2016 September 17
A convergent synthesis of one isomer of the C14-C29 fragment of mirabalin is disclosed. The key steps include a Marshall allenylation, a Mukaiyama aldol reaction and a Crimmins aldolization, which allow the control of 10 out of 25 stereogenic centers present in the molecule.

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