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Research Support, Non-U.S. Gov't
Research Support, U.S. Gov't, Non-P.H.S.
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Highly regioselective nitrile oxide dipolar cycloadditions with ortho-nitrophenyl alkynes.

Melissa L McIntosh, Michael R Naffziger, Bradley O Ashburn, Lev N Zakharov, Rich G Carter
Organic & Biomolecular Chemistry 2012 December 15
The dipolar cycloadditions of ortho-nitrophenyl alkynes with aryl nitrile oxides has been demonstrated. A range of substituents are tolerated on the alkyne. These reactions proceed with excellent levels of regioselectivity. Subsequent functionalization of the isoxazole scaffold has been demonstrated.

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