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Journal Article
Research Support, N.I.H., Extramural
Research Support, Non-U.S. Gov't
Dynamic nuclear polarization with a rigid biradical.
Angewandte Chemie 2009
A new polarizing agent with superior performance in dynamic nuclear polarization experiments is introduced, and utilizes two TEMPO (2,2,6,6-tetramethylpiperidine-1-oxyl) moieties connected through a rigid spiro tether (see structure). The observed NMR signal intensities were enhanced by a factor of 1.4 compared to those of TOTAPOL, a previously described TEMPO-based biradical with a flexible tether.
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