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https://www.readbyqxmd.com/read/28214442/hydrothermal-liquefaction-of-sewage-sludge-under-isothermal-and-fast-conditions
#1
Lili Qian, Shuzhong Wang, Phillip E Savage
We investigated the effects of water loading, sludge moisture content, recovery solvent, and additives on the product yields and compositions from isothermal (673K, 60min) and fast (773K, 1min) hydrothermal liquefaction (HTL) of sewage sludge. The water loading (which affects pressure within the reactor) plays a small role in product yields. The sludge moisture content had a larger effect with the highest biocrude yields (26.8wt% from isothermal HTL and 27.5wt% from fast HTL) being produced from sludge that was 85wt% moisture...
February 8, 2017: Bioresource Technology
https://www.readbyqxmd.com/read/28213709/high-efficiency-removal-of-triclosan-by-structure-directing-agent-modified-mesoporous-mil-53-al
#2
Rongni Dou, Junya Zhang, Yuancai Chen, Siyuan Feng
In order to expand the potential applications of metal-organic frameworks (MOFs), structure directing agents modified mesoporous MIL-53(Al) (MIL-53(Al)-1) was investigated to adsorb triclosan (TCS) with two different initial concentrations. MIL-53(Al)-1 with high mesoporosity and total pore volume exhibited higher adsorption capacity and 4.4 times faster adsorption of TCS at low concentration (1 mg L(-1)) than that of microporous MIL-53(Al). Also, mesoporous as well as microporous MIL-53(Al) showed significant higher adsorption capacity and two orders of magnitude greater fast uptake of TCS than two kinds of mesoporous-activated carbon...
February 18, 2017: Environmental Science and Pollution Research International
https://www.readbyqxmd.com/read/28213306/phosphorous-extractability-and-ryegrass-availability-from-bio-waste-composts-in-a-calcareous-soil
#3
Marco Grigatti, Elisa Boanini, Silvia Mancarella, Andrea Simoni, Massimo Centemero, Adrie H M Veeken
In this work four stable bio-waste composts (C1, C2, C3, C4) were selected on the basis of their increasing water soluble P (H2O-P). The P speciation was assessed via sequential chemical extraction (SCE) on the same products. Moreover, the plant-available P was assessed via apparent recovery fraction approach (ARF) in a pot test on ryegrass over 21 weeks at 15 mg P kg(-)(1) of soil. An inorganic P source (P-chem) was added as a reference at the same P rate in addition to a non-fertilized control (Control)...
February 6, 2017: Chemosphere
https://www.readbyqxmd.com/read/28213253/sensitive-kinetic-catalytic-spectrophotometric-method-for-cobalt-determination-using-a-chip-coupled-to-a-multisyringe-flow-injection-analysis-system
#4
Fatima Zohra Abouhiat, Camelia Henríquez, Farida El Yousfi, Víctor Cerdà
The development of an automated kinetic-catalytic spectrophotometric method for cobalt determination is presented. The method is based on the catalytic effect of Co in the oxidation of hydroxybenzoic acid by H2O2 in basic media. The method has been automated using a multisyringe flow injection system coupled to a monolithic flow conduit called chip (chip-MSFIA). All reagents and sample are simultaneously propelled into the chip to achieve an efficient mixing. The reaction product is monitored at 482nm. The reaction takes place very fast at room temperature, thus the fixed-time method is applied to quantify Co concentration in samples...
May 1, 2017: Talanta
https://www.readbyqxmd.com/read/28213238/preparation-and-evaluation-of-magnetic-core-shell-mesoporous-molecularly-imprinted-polymers-for-selective-adsorption-of-tetrabromobisphenol-s
#5
Xuemei Wang, Pengfei Huang, Xiaomin Ma, Huan Wang, Xiaoquan Lu, Xinzhen Du
Novel magnetic mesoporous molecularly imprinted polymers (MMIPs) with core-shell structure were prepared by simple surface molecular imprinting polymerization using tetrabromobisphenol-S (TBBPS) as the template. The MMIPs-TBBPS were characterized by fourier-transform infrared spectrometry (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), N2 adsorption-desorption transmission, and vibrating sample magnetometry. The resultant MMIPs-TBBPS were successfully applied magnetic solid-phase extraction (MSPE) coupled with HPLC determination of TBBPS in spiked real water samples with recoveries of 77...
May 1, 2017: Talanta
https://www.readbyqxmd.com/read/28213230/the-pentafluorophenyl-stationary-phase-shows-a-unique-separation-efficiency-for-performing-fast-chromatography-determination-of-highbush-blueberry-anthocyanins
#6
Barbora Šmídová, Dalibor Šatínský, Kateřina Dostálová, Petr Solich
A high-performance liquid chromatography method using an alternative pentafluorophenyl (PFP) core-shell stationary phase has been developed and used for rapid separation of 23 anthocyanins in a highbush blueberry Bluehaven cultivar. A high efficiency of separation of anthocyanins was achieved in the core-shell column Kinetex PFP, 150×4.6mm (particle size 2.6µm) with a 5×4.6mm precolumn, using a simple linear gradient elution with a mobile phase of acetonitrile and a water solution of 2% formic acid at a flow rate of 1...
May 1, 2017: Talanta
https://www.readbyqxmd.com/read/28213218/dynamic-flow-through-approach-to-evaluate-readily-bioaccessible-antioxidants-in-solid-food-samples
#7
Miguel A Maia, Tânia R P Soares, Ana I P Mota, María Rosende, Luís M Magalhães, Manuel Miró, Marcela A Segundo
Release of bioactive compounds from food matrices is regarded as the first step towards their human bioavailability. The objective of this work was the implementation of an affordable and robust flow-through device for expedient dynamic leaching experiments aiming at the assessment of readily bioaccessible antioxidant compounds in solid food commodities. A simple configuration is proposed using commercially available devices containing regenerated cellulose filters placed in polypropylene holders to entrap the solid sample, featuring a disposable, single use extraction chamber...
May 1, 2017: Talanta
https://www.readbyqxmd.com/read/28211324/aqueous-chlorination-of-fenamic-acids-kinetic-study-transformation-products-identification-and-toxicity-prediction
#8
Liyun Ma, Jian Li, Li Xu
Fenamic acids, one important type of non-steroidal anti-inflammatory drugs, are ubiquitous in environmental matrices. Thus it is of high significance to know the fate of them during chlorination disinfection considering their potential toxicity to the environment and humans. In the present study, the chlorination kinetics of three fenamic acids, i.e. mefenamic acid (MEF), tolfenamic acid (TOL) and clofenamic acid (CLO), were examined at different pHs, which followed second-order reaction under studied conditions...
February 8, 2017: Chemosphere
https://www.readbyqxmd.com/read/28211267/efficient-and-selective-uptake-of-tco4-by-a-cationic-metal-organic-framework-material-with-open-ag-sites
#9
Daopeng Sheng, Lin Zhu, Chao Xu, Chengliang Xiao, Yanlong Wang, Yaxing Wang, Lanhua Chen, Juan Diwu, Jing Chen, Zhifang Chai, Thomas E Albrecht-Schmitt, Shuao Wang
99Tc is one of the most problematic radioisotopes in used nuclear fuel owing to its combined features of high fission yield, long half-life, and high environmental mobility. There are only a handful of functional materials that can remove TcO4- anion from aqueous solution and identifying for new, stable materials with high anion-exchange capacities, fast kinetics, and good selectivity remains a challenge. We report here an 8-fold interpenetrated three-dimensional cationic metal-organic framework material, SCU-100, which is assembled from a tetradentate neutral nitrogen-donor ligand and two-coordinate Ag+ cations as potential open metal sites...
February 17, 2017: Environmental Science & Technology
https://www.readbyqxmd.com/read/28210946/an-online-spe-lc-ms-ms-method-for-the-analysis-of-antibiotics-in-environmental-water
#10
Meierjohann Axel, Kortesmäki Ewelina, Brozinski Jenny-Maria, Kronberg Leif
A fast and simple method for the analysis of 17 commonly used antibiotics in Finland in water samples was developed. The method combines online solid phase extraction using a reusable online trapping column combined with analytical separation on a C18 analytical column and detection by a triple quadrupole mass spectrometer. The method was fully validated for detection and quantification limits as well as linearity, repeatability, and matrix effects. The method gave an excellent linear response (r (2) > 0...
February 16, 2017: Environmental Science and Pollution Research International
https://www.readbyqxmd.com/read/28210347/assessing-cognitive-performance-in-badminton-players-a-reproducibility-and-validity-study
#11
Tanja van de Water, Barbara Huijgen, Irene Faber, Marije Elferink-Gemser
Fast reaction and good inhibitory control are associated with elite sports performance. To evaluate the reproducibility and validity of a newly developed Badminton Reaction Inhibition Test (BRIT), fifteen elite (25 ± 4 years) and nine non-elite (24 ± 4 years) Dutch male badminton players participated in the study. The BRIT measured four components: domain-general reaction time, badminton-specific reaction time, domain-general inhibitory control and badminton-specific inhibitory control. Five participants were retested within three weeks on the badminton-specific components...
January 1, 2017: Journal of Human Kinetics
https://www.readbyqxmd.com/read/28209247/water-hyacinth-a-potential-source-for-value-addition-an-overview
#12
REVIEW
Raveendran Sindhu, Parameswaran Binod, Ashok Pandey, Aravind Madhavan, Jose Anju Alphonsa, Narisetty Vivek, Edgard Gnansounou, Eulogio Castro, Vincenza Faraco
Water hyacinth a fresh water aquatic plant is considered as a noxious weed in many parts of the world since it grows very fast and depletes nutrients and oxygen from water bodies adversely affecting the growth of both plants and animals. Hence conversion of this problematic weed to value added chemicals and fuels helps in the self-sustainability especially for developing countries. The present review discusses the various value added products and fuels which can be produced from water hyacinth, the recent research and developmental activities on the bioconversion of water hyacinth for the production of fuels and value added products as well as its possibilities and challenges in commercialization...
January 25, 2017: Bioresource Technology
https://www.readbyqxmd.com/read/28208491/dynamic-shear-jamming-in-dense-granular-suspensions-under-extension
#13
Sayantan Majumdar, Ivo R Peters, Endao Han, Heinrich M Jaeger
Unlike dry granular materials, a dense granular suspension like cornstarch in water can strongly resist extensional flows. At low extension rates, such a suspension behaves like a viscous fluid, but rapid extension results in a response where stresses far exceed the predictions of lubrication hydrodynamics and capillarity. To understand this remarkable mechanical response, we experimentally measure the normal force imparted by a large bulk of the suspension on a plate moving vertically upward at a controlled velocity...
January 2017: Physical Review. E
https://www.readbyqxmd.com/read/28208212/the-function-of-the-ocelloid-and-piston-in-the-dinoflagellate-erythropsidinium-gymnodiniales-dinophyceae
#14
Fernando Gómez
The marine dinoflagellate Erythropsidinium possesses an ocelloid, the most elaborate photoreceptor organelle known in a unicellular organism, and a piston, a fast contractile appendage unknown in any other organism. The ocelloid is able to rotate, often before the cell swims. The ocelloid contains lenses that function to concentrate light. The flagellar propulsion is atrophied, and the piston is responsible for locomotion through successive extensions and contractions. During the 'locomotion mode', the contraction is ~4 times faster than the extension...
February 16, 2017: Journal of Phycology
https://www.readbyqxmd.com/read/28208062/nano-suspension-coating-as-a-technique-to-modulate-the-drug-release-from-controlled-porosity-osmotic-pumps-for-a-soluble-agent
#15
Leila Azharshekoufeh Bahari, Yousef Javadzadeh, Mohammad Barzegar Jalali, Peyvand Johari, Ali Nokhodchi, Javad Shokri
In controlled porosity osmotic pumps (CPOP), usually finding a single solvent with a capability to dissolve both film former (hydrophobic) and pore former (hydrophilic) is extremely challenging. Therefore, the aim of the present investigation was to tackle the issue associated with controlled porosity osmotic pump (CPOP) system using nano-suspension coating method. In the present study 4-Amino pyridine was used as a highly water soluble drug. In this method, a hydrophilic pore former (sucrose or mannitol) in nano range was suspended in polymeric coating solution using ball-mill...
February 8, 2017: Colloids and Surfaces. B, Biointerfaces
https://www.readbyqxmd.com/read/28207408/evaluation-of-cannabinoids-concentration-and-stability-in-standardized-preparations-of-cannabis-tea-and-cannabis-oil-by-ultra-high-performance-liquid-chromatography-tandem-mass-spectrometry
#16
Roberta Pacifici, Emilia Marchei, Francesco Salvatore, Luca Guandalini, Francesco Paolo Busardò, Simona Pichini
BACKGROUND: Cannabis has been used since ancient times to relieve neuropathic pain, to lower intraocular pressure, to increase appetite and finally to decrease nausea and vomiting. The combination of the psychoactive cannabis alkaloid Δ9-tetrahydrocannabinol (THC) with the non-psychotropic alkaloids cannabidiol (CBD) and cannabinol (CBN) demonstrated a higher activity than THC alone. The Italian National Institute of Health sought to establish conditions and indications on how to correctly use nationally produced cannabis to guarantee therapeutic continuity in individuals treated with medical cannabis...
February 16, 2017: Clinical Chemistry and Laboratory Medicine: CCLM
https://www.readbyqxmd.com/read/28205433/a-battery-operated-atomic-emission-analyzer-for-waterborne-arsenic-based-on-atmospheric-pressure-glow-discharge-excitation-source
#17
Chun Yang, Dong He, Zhenli Zhu, Huan Peng, Zhifu Liu, Guojun Wen, Jianghao Bai, Hongtao Zheng, Shenghong Hu, Yanxin Wang
In this paper, a sensitive atomic emission spectrometer (AES) based on a new low power and low argon consumption (< 8 W, 100 mL min(-1)) miniature direct current (DC) atmospheric pressure glow discharge (APGD) plasma (3 mm×5 mm) excitation source was developed for the determination of arsenic in water samples. In this method, arsenic in water was reduced to AsH3 by hydride generation (HG), which was then transported to the APGD source for excitation and detected by a compact CCD (charge-coupled device) microspectrometer...
February 16, 2017: Analytical Chemistry
https://www.readbyqxmd.com/read/28201912/free-energy-functionals-for-polarization-fluctuations-pekar-factor-revisited
#18
Mohammadhasan Dinpajooh, Marshall D Newton, Dmitry V Matyushov
The separation of slow nuclear and fast electronic polarization in problems related to electron mobility in polarizable media was considered by Pekar 70 years ago. Within dielectric continuum models, this separation leads to the Pekar factor in the free energy of solvation by the nuclear degrees of freedom. The main qualitative prediction of Pekar's perspective is a significant, by about a factor of two, drop of the nuclear solvation free energy compared to the total (electronic plus nuclear) free energy of solvation...
February 14, 2017: Journal of Chemical Physics
https://www.readbyqxmd.com/read/28198884/characterization-of-a-liquid-filled-nodeless-anti-resonant-fiber-for-biochemical-sensing
#19
Xiao-Lu Liu, Wei Ding, Ying-Ying Wang, Shou-Fei Gao, Ling Cao, Xian Feng, Pu Wang
We theoretically and experimentally characterize a liquid-filled nodeless anti-resonant fiber (LARF) that could find versatile applications in biochemical sensing. When a hollow-core nodeless anti-resonant fiber (HARF) is filled with a low refractive index liquid such as water or aqueous solutions in the whole hollow area, it preserves its anti-resonant reflection waveguiding mechanism with attributes encompassing the broad transmission bandwidth in UV, visible, and near IR; the neglectable confinement loss; and the acceptable single-mode quality...
February 15, 2017: Optics Letters
https://www.readbyqxmd.com/read/28196754/determination-of-groundwater-recharge-mechanism-in-the-deep-loessial-unsaturated-zone-by-environmental-tracers
#20
Zhi Li, Xi Chen, Wenzhao Liu, Bingcheng Si
Studying the groundwater recharge mechanism in regions with thick unsaturated zone can greatly improve our understanding of hydrological processes since these regions have complex groundwater processes. This study attempted to discuss the groundwater recharge in a region covered by loess over 130m deep in China's Loess Plateau. The water stable isotope, tritium and chloride in precipitation, groundwater and soil water were determined and used as inputs of mass balance methods. The tracer technique is found to be applicable and effective this region with thick unsaturated zone...
February 10, 2017: Science of the Total Environment
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