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https://www.readbyqxmd.com/read/28643123/study-of-the-interactions-of-dissolved-organic-matter-with-zinc-ion-and-the-impact-of-competitive-metal-ions-ca-2-and-mg-2-by-in-situ-absorbance
#1
Tianyu Zhang, Tao Wang, Yujuan Lu
The bioavailability and toxicity of zinc to aquatic life depend on dissolved organic matter (DOM), such as Suwannee River Fulvic Acid (SRFA), which plays an important role in the speciation of zinc. This study examined reactions of SRFA with zinc at different concentrations from pH 3.0 to 9.0, and competitive binding of calcium/magnesium and zinc to SRFA at pH 6.0, using in situ absorbance. Interactions of Zn(2+) with SRFA chromophores were evidenced by the emergence of features in Zn-differential spectra. Among all Zn(2+)-SRFA systems, dominant peaks, located at 235, 275 and 385 nm, and the highest intensity at 235 nm indicated the replacement of protons by the bound Zn(2+)...
June 22, 2017: Environmental Geochemistry and Health
https://www.readbyqxmd.com/read/28641186/composition-of-dissolved-organic-matter-dom-from-periodically-submerged-soils-in-the-three-gorges-reservoir-areas-as-determined-by-elemental-and-optical-analysis-infrared-spectroscopy-pyrolysis-gc-ms-and-thermally-assisted-hydrolysis-and-methylation
#2
Tao Jiang, Joeri Kaal, Jian Liang, Yaoling Zhang, Shiqiang Wei, Dingyong Wang, Nelson W Green
Soil-derived dissolved organic matter (DOM) has a major influence in biogeochemical processes related to contaminant dynamics and greenhouse gas emissions, due to its reactivity and its bridging role between the soil and aquatic systems. Within the Three Gorges Reservoir (TGR, China) area, an extensive water-fluctuation zone periodically submerges the surrounding soils. Here we report a characterization study of soil-derived DOM across the TGR areas, using elemental and optical analysis, infrared spectroscopy (FTIR), pyrolysis-GC-MS (Py-GC-MS) and thermally assisted hydrolysis and methylation (THM-GC-MS)...
June 19, 2017: Science of the Total Environment
https://www.readbyqxmd.com/read/28640201/deoxynivalenol-biomarkers-in-the-urine-of-uk-vegetarians
#3
Liz Wells, Laura Hardie, Courtney Williams, Kay White, Yunru Liu, Barbara De Santis, Francesca Debegnach, Georgio Moretti, Stephanie Greetham, Carlo Brera, Maria Papageorgiou, Natalie J Thatcher, Alan Rigby, Stephen L Atkin, Thozhukat Sathyapalan
Deoxynivalenol (DON) is produced by Fusarium graminearum and is one of the most commonly occurring trichothecenes. Vegetarians are alleged to be a high-risk group for DON exposure due to high intakes of cereals susceptible to the growth of the mycotoxin. This study provides the levels of DON and de-epoxi Deoxynivalenol (DOM-1) in urine analysed by liquid chromatography-mass spectrometry (LC-MS) in UK vegetarians. Over two consecutive days, morning urine samples were collected from 32 vegetarians and 31 UK adult volunteers, and associated food consumption 24 h prior to the sample was recorded...
June 22, 2017: Toxins
https://www.readbyqxmd.com/read/28638985/glucuronidation-of-deoxynivalenol-don-by-different-animal-species-identification-of-iso-don-glucuronides-and-iso-deepoxy-don-glucuronides-as-novel-don-metabolites-in-pigs-rats-mice-and-cows
#4
Heidi E Schwartz-Zimmermann, Christian Hametner, Veronika Nagl, Iris Fiby, Lukas Macheiner, Janine Winkler, Sven Dänicke, Erica Clark, James J Pestka, Franz Berthiller
The Fusarium mycotoxin deoxynivalenol (DON) is a frequent contaminant of cereal-based food and feed. Mammals metabolize DON by conjugation to glucuronic acid (GlcAc), the extent and regioselectivity of which is species-dependent. So far, only DON-3-glucuronide (DON-3-GlcAc) and DON-15-GlcAc have been unequivocally identified as mammalian DON glucuronides, and DON-7-GlcAc has been proposed as further DON metabolite. In the present work, qualitative HPLC-MS/MS analysis of urine samples of animals treated with DON (rats: 2 mg/kg bw, single bolus, gavage; mice: 1 mg/kg bw, single i...
June 21, 2017: Archives of Toxicology
https://www.readbyqxmd.com/read/28630573/effects-of-suspended-moxibustion-on-delayed-onset-muscle-soreness-a-randomized-controlled-double-blind-pilot-study
#5
Ding Meng, Dong Xiaosheng, Wang Xuhui, Wang Xu, Zhang Xijin
The objective of this study was to investigate the effects of suspended moxibustion upon tender point on delayed onset muscle soreness. The study was a randomized double-blind controlled trial with 50 subjects in each group. Subjects in moxibustion group received suspended moxibustion upon tender point (by palpation) twice. The controls received no treatment. Each subject received treatments twice, 24 hr and 48 hr after the delayed onset muscle soreness induction. The measurements of Pain Visual Analog Scale, maximum isometric muscle strength and circumference were made immediately after delayed onset muscle soreness induction, before and after every treatment session and 72 hr after delayed onset muscle soreness induction...
June 2017: Journal of Sports Science & Medicine
https://www.readbyqxmd.com/read/28628308/molecular-insights-into-the-transformation-of-dissolved-organic-matter-in-landfill-leachate-concentrate-during-biodegradation-and-coagulation-processes-using-esi-ft-icr-ms
#6
Ziwen Yuan, Chen He, Quan Shi, Chunming Xu, Zhenshan Li, Chengzhai Wang, Huazhang Zhao, Jinren Ni
Landfill leachate concentrate is a type of refractory organic wastewater with high environmental risk. Identification of refractory components and insights into the molecular transformations of the organics are essential for the development of efficient treatment process. In this report, molecular compositions of dissolved organic matter (DOM) in leachate concentrate, as well as changes after anaerobic/aerobic biodegradation and coagulation with salts, were characterized using electrospray ionization (ESI) coupled with Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS)...
June 19, 2017: Environmental Science & Technology
https://www.readbyqxmd.com/read/28627885/absolute-quantification-of-water-in-microporous-solids-with-1-h-mas-nmr-and-standard-addition
#7
Maarten Houlleberghs, Andreas Hoffmann, Dirk Dom, Christine E A Kirschhock, Francis Taulelle, Johan A Martens, Eric Breynaert
Zeolites are microporous materials driving industrial scale adsorption, ion exchange and catalytic processes. Their water content dramatically impacts their properties, but its quantification with Karl Fisher titration or thermal gravimetric analysis is problematic. Combining standard addition of water with 1H MAS NMR detection, absolute quantification of water in microporous materials becomes possible. The method was demonstrated on 5 different, commercially available zeolites.
June 19, 2017: Analytical Chemistry
https://www.readbyqxmd.com/read/28627273/nanoparticle-interactions-with-co-existing-contaminants-joint-toxicity-bioaccumulation-and-risk
#8
Rui Deng, Daohui Lin, Lizhong Zhu, Sanghamitra Majumdar, Jason C White, Jorge L Gardea-Torresdey, Baoshan Xing
With their growing production and application, engineered nanoparticles (NPs) are increasingly discharged into the environment. The released NPs can potentially interact with pre-existing contaminants, leading to biological effects (bioaccumulation and/or toxicity) that are poorly understood. Most studies on NPs focus on single analyte exposure; the existing literature on joint toxicity of NPs and co-existing contaminants is rather limited but beginning to develop rapidly. This is the first review paper evaluating the current state of knowledge regarding the joint effects of NPs and co-contaminants...
June 19, 2017: Nanotoxicology
https://www.readbyqxmd.com/read/28625121/nanofiltration-fouling-propensity-caused-by-wastewater-effluent-organic-matters-and-surface-water-dissolved-organic-matters
#9
Wentao Shang, Feiyun Sun, Lichun Chen
Rejection of dissolved organic matters (DOM) from wastewater treatment plant effluent (EfOM) and surface reservoir water (RW-DOM) by nanofiltration (NF) was comparatively studied to evaluate their influence on membrane fouling, and to unveil the major causations. EfOM and RW-DOM were fractionated to determine the major components that preferentially form fouling layer and initiate biofouling. The results indicated that EfOM induced a rapid membrane permeability loss and a more complicated biofilm diversity than RW-DOM did...
June 19, 2017: Environmental Technology
https://www.readbyqxmd.com/read/28624634/impact-of-upgrading-wastewater-treatment-plant-on-the-removal-of-typical-methyl-oxygenated-chlorinated-and-parent-polycyclic-aromatic-hydrocarbons
#10
Meng Qiao, Wei Cao, Bochuan Liu, Yaohui Bai, Weixiao Qi, Xu Zhao, Jiuhui Qu
Wastewater treatment plant (WWTP) secondary effluent is a main source for polycyclic aromatic hydrocarbons (PAHs) and their derivatives (SPAHs) to wastewater receiving rivers in Beijing. The treatment technologies are being upgraded in the WWTPs as the tertiary treatment. To assess the improvement of the removal efficiencies of PAHs and SPAHs after the treatment upgrading, we investigated 16 PAHs and 4 types of SPAHs in the secondary and tertiary treatment process in 5 major WWTPs. Most of the parent PAHs, methyl PAHs, oxygenated PAHs and chlorinated PAHs were detected in the influent, secondary and tertiary effluent...
June 14, 2017: Science of the Total Environment
https://www.readbyqxmd.com/read/28623827/changes-in-aquatic-microbial-responses-to-c-substrates-with-stream-water-and-sediment-quality-related-to-land-use-pressures
#11
Marc I Stutter, Jonathan Cains
The degradation of aquatic ecosystems by multiply-acting stressors is a key threat requiring new approaches to identify impairment processes and restoration targets. Heterotrophic respiration of C-substrates can be an integrative indicator of how aquatic ecosystems respond to pollution. We utilised sixteen C-substrates (simple metabolites to dissolved organic matter (DOM)) to characterise substrate induced respiration (SIR) for sediments from sixteen NE Scotland streams covering a range of land use-related pollution pressures...
June 8, 2017: Chemosphere
https://www.readbyqxmd.com/read/28620853/effects-of-ozonation-powdered-activated-carbon-adsorption-and-coagulation-on-the-removal-of-disinfection-by-product-precursors-in-reservoir-water
#12
Feng Wang, Baoyu Gao, Qinyan Yue, Fan Bu, Xue Shen
Effects of ozonation and powdered activated carbon on removal of dissolved organic matter (DOM) and disinfection by-product (DBP) in reservoir water were intensively investigated in this study. Both the formation of carbonaceous DBP (C-DBP) and nitrogenous DBP (N-DBP) as well as their speciation were analyzed. Results exhibited that the addition of powdered activated carbon (PAC) greatly improved the removal of aromatic protein. Trihalomethanes (THMs) and haloacetonitriles (HANs) were the dominant species in C-DBP and N-DBP...
June 15, 2017: Environmental Science and Pollution Research International
https://www.readbyqxmd.com/read/28618358/identifying-structural-characteristics-of-humic-acid-to-static-and-dynamic-fluorescence-quenching-of-phenanthrene-9-phenanthrol-and-naphthalene
#13
Lin Wang, Hao Li, Yu Yang, Di Zhang, Min Wu, Bo Pan, Baoshan Xing
Fluorescence quenching is a sensitive and fast method to quantify the interactions between a fluorescent organic contaminant and a quencher, such as dissolved organic matter (DOM). Dynamic fluorescence quenching is resulted from molecular collision, not the real binding, and thus it complicates the binding data interpretation. On the other hand, static fluorescence quenching occurs for fluorescent contaminants of ground states, which decreases the concentration of freely dissolved contaminants. However, how a particular structure in DOM contributes to the static and dynamic fluorescence quenching of a fluorescent contaminant is still unclear, which has greatly hindered the application of fluorescence quenching technique...
June 12, 2017: Water Research
https://www.readbyqxmd.com/read/28618153/cascading-influence-of-inorganic-nitrogen-sources-on-dom-production-composition-lability-and-microbial-community-structure-in-the-open-ocean
#14
S J Goldberg, C E Nelson, D A Viviani, C N Shulse, M J Church
Nitrogen frequently limits oceanic photosynthesis and the availability of inorganic nitrogen sources in the surface oceans is shifting with global change. We evaluated the potential for abrupt increases in inorganic N sources to induce cascading effects on DOM and microbial communities in the surface ocean. We collected water from 5 m depth in the central North Pacific and amended duplicate 20 L polycarbonate carboys with nitrate or ammonium, tracking planktonic carbon fixation, DOM production, DOM composition and microbial community structure responses over 1 week relative to controls...
June 15, 2017: Environmental Microbiology
https://www.readbyqxmd.com/read/28614163/effect-of-low-volume-high-intensity-interval-exercise-and-continuous-exercise-on-delayed-onset-muscle-soreness-in-untrained-healthy-males
#15
Luiz F Farias Junior, Rodrigo A V Browne, Danniel T Frazão, Teresa C B Dantas, Paulo H M Silva, Rodrigo P A Freitas, Marcelo S Aoki, Eduardo C Costa
The aim of this study was to compare the effect of a single session of a low-volume high-intensity interval exercise (HIIE) and a continuous exercise (CE) on the magnitude of delayed onset-muscle soreness (DOMS) in untrained healthy males. Fifteen participants (25.1±4.4 years) completed 2 experimental sessions in a randomized order: (a) low-volume HIIE: 10 x 60 s at 90% of maximal velocity (MV) interspersed with 60s of active recovery at 30% of MV; and (b) CE: 20 min at 60% of MV. Pressure-pain threshold (PPT), pressure-pain tolerance (PPTol) and perceived pain intensity (PPI) were assessed in the rectus femoris, biceps femoris and gastrocnemius before and 24 hours post-exercise...
June 12, 2017: Journal of Strength and Conditioning Research
https://www.readbyqxmd.com/read/28611434/linking-optical-and-molecular-signatures-of-dissolved-organic-matter-in-the-mediterranean-sea
#16
Alba María Martínez-Pérez, Mar Nieto-Cid, Helena Osterholz, Teresa S Catalá, Isabel Reche, Thorsten Dittmar, Xosé Antón Álvarez-Salgado
Dissolved organic matter (DOM) plays a key role in global biogeochemical cycles and experiences changes in molecular composition as it undergoes processing. In the semi-closed basins of the oligotrophic Mediterranean Sea, these gradual molecular modifications can be observed in close proximity. In order to extend the spatial resolution of information on DOM molecular composition available from ultrahigh resolution mass spectrometry in this area, we relate this data to optical (fluorescence and absorption spectroscopy) measurements...
June 13, 2017: Scientific Reports
https://www.readbyqxmd.com/read/28606809/animal-derived-natural-products-used-in-the-bhutanese-sowa-riga-medicine
#17
Karma Yeshi, Paolo Morisco, Phurpa Wangchuk
ETHNOPHARMACOLOGICAL RELEVANCE: Bhutan has two traditional healing systems: a folklore medicine and the Bhutanese Sowa Rigpa medicine (BSM). Three different types of ingredients namely plants, animals (and their derived products) and minerals are used for the preparation of various formulations in combined form. Animals and their derived products are vital ingredients in the preparation of numerous traditional remedies. Unlike medicinal plants, research on medicinal animals has remained largely untouched...
June 9, 2017: Journal of Ethnopharmacology
https://www.readbyqxmd.com/read/28603977/parafac-modeling-of-irradiation-and-oxidation-induced-changes-in-fluorescent-dissolved-organic-matter-extracted-from-poultry-litter
#18
Kiranmayi P Mangalgiri, Stephen Andrew Timko, Michael Gonsior, Lee Blaney
Parallel factor analysis (PARAFAC) allows quantitative assessment of the composition of fluorescent dissolved organic matter (DOM). In this study, we developed a 4-component PARAFAC model to characterize DOM extracted from poultry litter. The dataset included fluorescence excitation-emission matrices from 291 untreated, irradiated (253.7 nm, 310 - 410 nm), and oxidized (UV-H2O2, ozone) poultry litter extracts. The four components were identified as microbial humic-, terrestrial humic-, tyrosine-, and tryptophan-like fluorescent signatures...
June 12, 2017: Environmental Science & Technology
https://www.readbyqxmd.com/read/28595855/dissociated-time-course-between-peak-torque-and-total-work-recovery-following-bench-press-training-in-resistance-trained-men
#19
Diogo V Ferreira, Paulo Gentil, João B Ferreira-Junior, Saulo R S Soares, Lee E Brown, Martim Bottaro
OBJECTIVE: To evaluate the time course of peak torque and total work recovery after a resistance training session involving the bench press exercise. DESIGN: Repeated measures with a within subject design. METHODS: Twenty-six resistance-trained men (age: 23.7±3.7years; height: 176.0±5.7cm; mass: 79.65±7.61kg) performed one session involving eight sets of the bench press exercise performed to momentary muscle failure with 2-min rest between sets...
June 7, 2017: Physiology & Behavior
https://www.readbyqxmd.com/read/28591660/the-effect-of-advanced-secondary-municipal-wastewater-treatment-on-the-molecular-composition-of-dissolved-organic-matter
#20
Andrew C Maizel, Christina K Remucal
There is a growing interest in water reuse and in recovery of nutrients from wastewater. Because many advanced treatment processes are designed to remove organic matter, a better understanding of the composition of dissolved organic matter (DOM) in wastewater is needed. To that end, we assessed DOM in the Nine Springs Wastewater Treatment Plant in Madison, Wisconsin by UV-visible spectroscopy and Fourier transform-ion cyclotron resonance mass spectrometry. Samples were collected from the influent and effluent of two different secondary treatment processes and their respective secondary clarifiers, the UV disinfection unit, and an Ostara treatment system, which produces struvite via chemical precipitation...
May 26, 2017: Water Research
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