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https://www.readbyqxmd.com/read/28922607/antdas-automatic-data-analysis-strategy-for-uplc-qtof-based-nontargeted-metabolic-profiling-analysis
#1
Hai-Yan Fu, Xiao-Ming Guo, Yue-Ming Zhang, Jing-Jing Song, Qing-Xia Zheng, Ping-Ping Liu, Peng Lu, Qian-Si Chen, Yong-Jie Yu, Yuanbin She
High-quality data analysis methodology remains a bottleneck for metabolic profiling analysis based on ultra-performance liquid chromatography-quadrupole time-of-flight mass spectrometry. The present work aims to address this problem by proposing a novel data analysis strategy wherein (1) chromatographic peaks in the UPLC-QTOF dataset are automatically extracted by using an advanced multiscale Gaussian smoothing-based peak extraction strategy. (2) A peak annotation stage is used to cluster fragment ions that belong to the same compound...
September 18, 2017: Analytical Chemistry
https://www.readbyqxmd.com/read/28920895/matched-filtering-for-heart-rate-estimation-on-compressive-sensing-ecg-measurements
#2
Giulia Da Poian, Christopher J Rozell, Riccardo Bernardini, Roberto Rinaldo, Gari D Clifford
OBJECTIVE: Compressive Sensing (CS) has recently been applied as a low complexity compression framework for long-term monitoring of electrocardiogram signals using Wireless Body Sensor Networks. Long-term recording of ECG signals can be useful for diagnostic purposes and to monitor the evolution of several widespread diseases. In particular, beat to beat intervals provide important clinical information, and these can be derived from the ECG signal by computing the distance between QRS complexes (R-peaks)...
September 14, 2017: IEEE Transactions on Bio-medical Engineering
https://www.readbyqxmd.com/read/28920796/successful-laparoscopic-oviductal-artificial-insemination-in-the-clouded-leopard-neofelis-nebulosa-in-thailand
#3
Wanlaya Tipkantha, Paweena Thuwanut, Umaporn Maikeaw, Ampika Thongphakdee, Saifon Yapila, Sumate Kamolnorranath, Boripat Siriaroonrat, Pierre Comizzoli, Kaywalee Chatdarong
Captive breeding of clouded leopards (Neofelis nebulosa) is challenging because of mating incompatibility, high incidence of teratospermia in males, and inconsistent ovulation patterns in females. Assisted reproductive techniques, therefore, are necessary to overcome these issues and maintain the genetic diversity in the captive population. The objective was to use laparoscopic oviductal artificial insemination (AI) to breed genetically valuable females (n = 4; aged 4.5-5 yr) that were unsuccessfully paired...
September 2017: Journal of Zoo and Wildlife Medicine: Official Publication of the American Association of Zoo Veterinarians
https://www.readbyqxmd.com/read/28920769/modacrylic-anion-exchange-fibers-for-cr-vi-removal-from-chromium-plating-rinse-water-in-batch-and-flow-through-column-experiments
#4
Seung-Chan Lee, Jin-Kyu Kang, Eun-Hye Sim, Nag-Choul Choi, Song-Bae Kim
The aim of this study was to investigate Cr(VI) removal from chromium-plating rinse water using modacrylic anion-exchange fibers (KaracaronTM KC31). Batch experiments were performed with synthetic Cr(VI) solutions to characterize the KC31 fibers in Cr(VI) removal. Cr(VI) removal by the fibers was affected by solution pH; the Cr(VI) removal capacity was the highest at pH 2 and decreased gradually with a pH increase from 2 to 12. In regeneration and reuse experiments, the Cr(VI) removal capacity remained above 37...
September 18, 2017: Journal of Environmental Science and Health. Part A, Toxic/hazardous Substances & Environmental Engineering
https://www.readbyqxmd.com/read/28920442/novelty-of-dynamic-process-in-the-synthesis-of-biocompatible-silica-nanotubes-by-biomimetic-glycyldodecylamide-as-a-soft-template
#5
Hyejung Choi, Joong-Jo Kim, Yong-Hwan Mo, Benjaram Mahipal Reddy
Dynamic process in the synthesis of silica nanotubes (SNTs) by utilizing glycyldodecylamide (GDA) as a soft template was thoroughly investigated. The morphological evolution from GDA to SNTs was deeply explored to elucidate the formation mechanism for optimizing the synthesis procedure. Various analytical tools, namely, XRD, FTIR, SEM, TEM, Z-potential, and N2 adsorption/desorption isotherms were employed during the synthesis procedure. The interactive structure of GDA was also investigated using TEM-EDX as a function of aging time...
September 18, 2017: Langmuir: the ACS Journal of Surfaces and Colloids
https://www.readbyqxmd.com/read/28919177/effects-of-gnrhr-polymorphisms-on-sperm-quality-in-chinese-water-buffalo
#6
Gang Wang, Linlin Hao, Yunyun Cheng, Shuai Li, Yu Zhang, Chen Lv, Wenzhen Wei, Shan Huang, Hongyu Shi, Lijie Dong, Yifan Zhang, Hao Yu, Jiabao Zhang
Gonadotropin-releasing hormone receptor (GnRHR) plays a critical physiological role in animal reproduction and is a potential marker for improving sperm quality. In the present study, eight SNPs (g.539T>C, g.640A>G, g.655T>C, g.707T>C, g.812A>G, g.18951A>T g.16867T>C and g.18953Indel GGCAAAGTAA) were detected in the GnRHR gene from one-hundred-sixty-five water buffalo by direct sequencing and identification of overlapping peaks. All SNPs were associated significantly with the ejaculate volume and two genes (g...
September 5, 2017: Animal Reproduction Science
https://www.readbyqxmd.com/read/28918325/a-novel-lc-ms-ms-method-for-the-quantitative-measurement-of-the-acetate-content-in-pharmaceutical-peptides
#7
Rani J Qasem, Ibrahim K Farh, Mohammed A Al Essa
Most pharmaceutical peptides are supplied as acetate salts and the relative amount of acetate to peptide in the final product is one quality criterion required by regulatory agencies to approve the product for clinical use. The objective of the present study was to develop a validated LC-MS/MS method that allows the quantitative determination of the acetate content in pharmaceutical peptide preparations and simultaneous monitoring and collection of qualitative and quantitative information on the peptide during manufacture and in the final product...
September 6, 2017: Journal of Pharmaceutical and Biomedical Analysis
https://www.readbyqxmd.com/read/28918220/synthesis-and-application-of-a-highly-selective-copper-ions-fluorescent-probe-based-on-the-coumarin-group
#8
Guangjie He, Xiangli Liu, Jinhe Xu, Liguo Ji, Linlin Yang, Aiying Fan, Songjun Wang, Qingzhi Wang
A highly selective copper ions fluorescent probe based on the coumarin-type Schiff base derivative 1 (probe) was produced by condensation reaction between coumarin carbohydrazide and 1H-indazole-3-carbaldehyde. The UV-vis spectroscopy showed that the maximum absorption peak of compound 1 appeared at 439nm. In the presence of Cu(2+) ions, the maximum peak decreased remarkably compared with other physiological important metal ions and a new absorption peak at 500nm appeared. The job's plot experiments showed that complexes of 1:2 binding mode were formed in CH3CN:HEPES (3:2, v/v) solution...
September 13, 2017: Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy
https://www.readbyqxmd.com/read/28918214/efficient-noise-tolerant-estimation-of-heart-rate-variability-using-single-channel-photoplethysmography
#9
Reza Firoozabadi, Eric D Helfenbein, Saeed Babaeizadeh
BACKGROUND: The feasibility of using photoplethysmography (PPG) for estimating heart rate variability (HRV) has been the subject of many recent studies with contradicting results. Accurate measurement of cardiac cycles is more challenging in PPG than ECG due to its inherent characteristics. METHODS: We developed a PPG-only algorithm by computing a robust set of medians of the interbeat intervals between adjacent peaks, upslopes, and troughs. Abnormal intervals are detected and excluded by applying our criteria...
August 18, 2017: Journal of Electrocardiology
https://www.readbyqxmd.com/read/28917797/a-rapid-and-specific-colorimetric-method-for-free-tryptophan-quantification
#10
Yinan Wu, Tianmin Wang, Chong Zhang, Xin-Hui Xing
Tryptophan is one of the eight essential amino acids and plays an important role in many biological processes. For its interaction with human health, environment and relevant commercial interest in biotechnology-based production, rapid and specific quantification method for this molecule accessible to common laboratories is badly needed. We herein reported a simple colorimetric method for free tryptophan quantification with 96-well-plate-level throughput. Our protocol firstly converted tryptophan to indole enzymatically by purified tryptophanases and then used reactivity of indole with hydroxylamine to form pink product with absorption peak at 530nm, enabling the quantification of tryptophan with simple spectrometry in just two hours...
January 1, 2018: Talanta
https://www.readbyqxmd.com/read/28917783/intellectual-modifying-a-bare-glassy-carbon-electrode-to-fabricate-a-novel-and-ultrasensitive-electrochemical-biosensor-application-to-determination-of-acrylamide-in-food-samples
#11
Kambiz Varmira, Omid Abdi, Mohammad-Bagher Gholivand, Hector C Goicoechea, Ali R Jalalvand
Acrylamide (AA) is a neurotoxin and carcinogen which is mainly formed in foods containing large quantities of starch processed at high temperatures and its determination is very important to control the quality of foods. In this work, a novel electrochemical biosensor based on hemoglobin-dimethyldioctadecylammonium bromide (HG-DDAB)/platinum-gold-palladium three metallic alloy nanoparticles (PtAuPd NPs)/chitosan-1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide (Ch-IL)/multiwalled carbon nanotubes-IL (MWCNTs-IL)/glassy carbon electrode (GCE) is proposed for ultrasensitive determination of AA in food samples...
January 1, 2018: Talanta
https://www.readbyqxmd.com/read/28917775/fabrication-of-bi-monomer-copolymer-of-pyrrole-indole-for-highly-efficient-solid-phase-microextraction-of-benzene-derivatives
#12
Jie Zhang, Baizhao Zeng, Faqiong Zhao
A procedure for direct electrochemical deposition of poly(pyrrole-indole) on gold nanoparticles coated stainless steel wire was established, and the formation of copolymer was confirmed by infrared spectroscopy. The synthesized coating showed unique microstructure, excellent extraction efficiency (2-10 times of corresponding single-component coating), high thermal stability (up to 280°C) and good durability (could be used for more than 200 times). As a novel and promising extraction coating, it was used for the headspace solid phase microextraction-gas chromatography detection of some benzene derivatives, including chlorobenzene, bromobenzene, p-bromotoluene, m-nitrotoluene and p-nitrotoluene...
January 1, 2018: Talanta
https://www.readbyqxmd.com/read/28917752/facilely-self-assembled-magnetic-nanoparticles-aptamer-carbon-dots-nanocomposites-for-highly-sensitive-up-conversion-fluorescence-turn-on-detection-of-tetrodotoxin
#13
Hui Jin, Rijun Gui, Jie Sun, Yanfeng Wang
In this work, magnetic Fe3O4 nanoparticles (NPs) were modified with aptamer of tetrodotoxin (TTX) to form Fe3O4/aptamer complex. The self-assembling of carbon dots (CDs) and the aptamer generated Fe3O4/aptamer/CDs nanocomposites. The nanocomposites exhibited down-conversion fluorescence and up-conversion fluorescence (UCF) emissions simultaneously. When excited at a wavelength of 780nm, the UCF (peaked at 475nm) of nanocomposites increased regularly with the increase of TTX concentration [TTX]. In the [TTX] range from 0...
January 1, 2018: Talanta
https://www.readbyqxmd.com/read/28917748/selectivity-improvement-of-positive-photoionization-ion-mobility-spectrometry-for-rapid-detection-of-organophosphorus-pesticides-by-switching-dopant-concentration
#14
Qinghua Zhou, Jia Li, Bin Wang, Shuang Wang, Haiyang Li, Jinyuan Chen
Ion mobility spectrometry (IMS) opened a potential avenue for the rapid detection of organophosphorus pesticides (OPPs), though an improved selectivity of stand-alone IMS was still in high demand. In this study, a stand-alone positive photoionization ion mobility spectrometry (PP-IMS) apparatus was constructed for the rapid detection of OPPs with acetone as dopant. The photoionization of acetone molecules was induced by the ultraviolet irradiation to produce the reactant ions (Ac)2H(+), which were employed to ionize the OPPs including fenthion, imidan, phosphamidon, dursban, dimethoate and isocarbophos via the proton transfer reaction...
January 1, 2018: Talanta
https://www.readbyqxmd.com/read/28917742/analysis-of-glutathione-in-the-presence-of-acetaminophen-and-tyrosine-via-an-amplified-electrode-with-mgo-swcnts-as-a-sensor-in-the-hemolyzed-erythrocyte
#15
Fahimeh Tahernejad-Javazmi, Mehdi Shabani-Nooshabadi, Hassan Karimi-Maleh
In this study, we investigated the effect of adding MgO/SWCNTs and 2-Chloro-N'-[1-(2,5-dihydroxyphenyl) methylidene]aniline (2-CDHPMA) to a carbon paste matrix, which could act as a voltammetric sensor for the analysis of glutathione. The electrocatalytic interaction between 2-CDHPMA and glutathione was used as a factor for the analysis of this biological compound in real samples. In addition, the presence of MgO/SWCNTs can help in increasing the sensitivity of the fabricated sensor and for obtaining a low limit of detection in the analysis of glutathione...
January 1, 2018: Talanta
https://www.readbyqxmd.com/read/28917172/reconstruction-of-atmospheric-trace-metals-pollution-in-southwest-china-using-sediments-from-a-large-and-deep-alpine-lake-historical-trends-sources-and-sediment-focusing
#16
Qi Lin, Enfeng Liu, Enlou Zhang, Bibhash Nath, Ji Shen, Hezhong Yuan, Rong Wang
Atmospheric pollution, one of the leading environmental problems in South and East Asia, and its impact on the terrestrial environmental quality remain poorly understood particularly in alpine areas where both historical and present-day mining and smelting operations might leave an imprint. Here, we reconstructed atmospheric trace metals pollution during the past century using core sediments from a large and deep alpine lake in Southwest China. The implication of in lake and/or in watershed sediment focusing in pollution quantification is discussed by analyzing 15 sediment cores...
September 13, 2017: Science of the Total Environment
https://www.readbyqxmd.com/read/28915937/ultra-high-performance-supercritical-fluid-chromatography-mass-spectrometry-procedure-for-analysis-of-monosaccharides-from-plant-gum-binders
#17
Volodymyr Pauk, Tomáš Pluháček, Vladimír Havlíček, Karel Lemr
The ultra-high performance supercritical fluid chromatography-mass spectrometry (UHPSFC/MS) procedure for analysis of native monosaccharides was developed. Chromatographic conditions were investigated to separate a mixture of four hexoses, three pentoses, two deoxyhexoses and two uronic acids. Increasing water content in methanol modifier to 5% and formic acid to 4% improved peak shapes of neutral monosaccharides and allowed complete elution of highly polar uronic acids in a single run. An Acquity HSS C18SB column outperformed other three tested stationary phases (BEH (silica), BEH 2-ethylpyridine, CSH Fluoro-Phenyl) in terms of separation of isomers and analysis time (4...
October 9, 2017: Analytica Chimica Acta
https://www.readbyqxmd.com/read/28915467/the-broad-emission-at-785nm-in-yag-ce-3-cr-3-phosphor
#18
Xianju Zhou, Xiaoxia Luo, Bing Wu, Sha Jiang, Li Li, Xiaobing Luo, Yu Pang
Luminescence of defects and/or impurities is important for phosphors. One broad emission band centered at 785nm was observed in (Y0.97Ce0.03)3(Al1-xCrx)5O12 (x=0.005, 0.01, 0.03, 0.06, 0.09), (YAG:Ce,Cr) nano-particles synthesized by polymer-assisted sol-gel method in this work. In order to study the source of this wide emission band, the crystalline phase structure of the phosphors was examined by X-ray diffraction (XRD). No obvious diffraction peaks due to impurity phase were observed even though the calcining temperature of the samples arrived at 1400°C...
September 8, 2017: Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy
https://www.readbyqxmd.com/read/28914777/the-usefulness-of-contrast-enhanced-ultrasound-in-the-assessment-of-early-kidney-transplant-function-and-complications
#19
REVIEW
Sara Álvarez Rodríguez, Vital Hevia Palacios, Enrique Sanz Mayayo, Victoria Gómez Dos Santos, Víctor Díez Nicolás, María Dolores Sánchez Gallego, Javier Lorca Álvaro, Francisco Javier Burgos Revilla
OBJECTIVES: The routine diagnostic method for assessment of renal graft dysfunction is Doppler ultrasound. However, contrast-enhanced ultrasound (CEUS) may provide more information about parenchymal flow and vascular status of kidney allografts. The aim of the study was to assess the effectiveness of CEUS in the immediate post-transplant period, focusing on acute vascular complications. A brief review of available literature and a report of our initial experience is made. MATERIAL AND METHODS: 15 kidney transplant (KT) cases with clinical suspicion of acute surgical complication were assessed with CEUS and conventional Doppler ultrasound (US)...
September 15, 2017: Diagnostics
https://www.readbyqxmd.com/read/28914691/time-trends-and-spatial-patterns-in-the-mesothelioma-incidence-in-slovenia-1961-2014
#20
Vesna Zadnik, Maja Primic Zakelj, Katja Jarm, Tina Zagar
We aimed to explore the temporal and spatial variations in mesothelioma incidence in Slovenia for the last 50 years and, among these, to evaluate the consequences of asbestos usage. The incidence data from the population-based Cancer Registry of Republic of Slovenia for the period 1961-2014 were analysed. The data of asbestos imported to Slovenia were used as a proxy for asbestos exposure in manufacturing areas. Log-linear joinpoint regression and age-period-cohort Poisson models were used in the time-trend analysis...
September 2017: European Journal of Cancer Prevention
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